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By T. Fleming, D. Harrington
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During the second, an aqueous ammonia reagent was added which did neutralize the solution. Heating and mixing were then stopped and the solution was allowed to settle. After about 3 hours, at 00:15 on 7 September, the criticality alarm sounded, and personnel promptly evacuated to the predetermined assembly location, an underground tunnel. Here it was determined (by the absence of blood sodium activation) that no one received a significant dose. The excursion may have fortuitously occurred while the operators were on a work break.
They were spaced a maximum of 30 m apart but were commonly much closer. 2 R/h. 8 R/h. Ultimately it was determined that there had been a total of 1,324 g of plutonium in the dissolution vessel at the time of the accident. This was about three times the criticality safety limit. The recovered nitric solution contained 933 g of plutonium and a very rich precipitate was found in the bottom of vessel 2. It contained 391 g of plutonium in 660 g of solids; the remainder was mostly graphite pulp from molds.
The plutonium in R2 was then precipitated with approximately 15 g of plutonium discharged with the supematant. The precipitate was again dissolved, and the carbonate solution was transferred to the holding vessel, leading to the criticality accident. Table 5. 0 Running Plutonium 9. total of in RO (g) 267–51 =216 216+ 176–21 =371 371 +328–39=660 660 +46 -24 = 682 8. Idaho Chemical Processing Plant, 25 January 196114115~1G~17 Uranyl nitrate solution, U(90), in a vapor disengagement This accident occurred in the main process building, CPP 601, in H-cel[, where fission products were chemically separated from dissolved spent fuel.